This section is intended to provide an overview of solid state NMR for someone unfamiliar with NMR techniques. For a more comprehensive theoretical explanation of NMR we recommend a few web resources on NMR and EPR which can be particularly useful due to their conciseness and clarity. Lastly we have recommended additional books at the bottom that are worth referencing.
General audiences are often unfamiliar with NMR, but frequently familiar with both cookies and guitars. The following description of NMR is one possible example of breaking down some of the complexities of the technique to the general public in a way that both catches some attention and explains the basic concept.
The LibreText NMR theory page provides a good introduction to the nuclear physicis that result in NMR
The LibreText Solid State Experiments page
provides a good explanation of Magic Angle Spinning and discussion of pulse sequences commonly used in solids NMR.
Glenn Facey's University of Ottawa NMR Facility Web Site is a treasure trove of answers to NMR questions.
Pascal Man's Personal Web site includes a large collection of inorganic solids NMR papers
For an in-depth discussion of the theory see our Paramagnetic Theory Page
Paramagnetic NMR utilizes a phenomenon where unpaired electron spins within a molecule or crystal interact with local nuclear spins. NMR spectra of nuclei which are close enough to the unpaired electron spins can be significantly altered.
The following books and other resources are listed as good references for obtaining or furthering an understanding of solid state NMR. We divide these resources into three audiences: Beginner, Moderate, and Advanced.
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Current Developments in Solid State NMR Spectroscopy, by Moller and Madhu 2003 Advanced level Publisher webpage for this bookThis is a descriptive book that has the level of detail leaving an expert satisfied, but overwhelming the novice. Its initial chapters are especially good references when returning to the theory after a few years of running NMR experiments. The price tag is high depending on where you purchase this, however it is often included in springer online access for direct download, so you may already have access to it though a universities web subscription. |
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Solid State NMR Spectroscopy, by Melinda Duer 2005 Middle level Publisher webpage for this bookThis is a good middle level book on a number of SSNMR topics, with a detail level that works well for a 2-3 year graduate student. The book cover links to the publishers website, however copies of this book are available for a cheaper price on other websites. |
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Spin Dynamics, by Malcolm H. Levitt 2008 Beginner level Publisher webpage for this bookThis book provides a good fundamental introduction to the physics and theory behind NMR in general. Although not specifically about solid state NMR it does include discussion on solids topics and presenting a general intoduction. The focus on liquids NMR may help scientsits new to solid state NMR make connections with material they have seen previously. |